化工社化工社 化学情報印刷レポート · 研究参考用
Trifluoroacetic acid → Butyltin trichloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Trifluoroacetic acid | HCID 6422 | — |
| 反応物 | Butyltin trichloride | HCID 14236 | — |
| 反応物 | Sodium | HCID 5360545 | — |
| 生成物 | Butyltin trichloride | HCID 14236 | — |
| 生成物 | Monobutyldichlorotin trifluoroacetate | HCID 20148371 | — |
反応手順
A reaction mixture of monobutyltin trichloride (200 g., 0.7 moles) and the sodium salt of trifluoroacetic acid (10 g., 0.07 moles) were heated at 70° C. for 3 hours and allowed to stand overnight at room temperature. The sodium chloride by-product and unreacted sodium salt were filtered. A liquid coating composition of about 12 wt.% monobutyldichlorotin trifluoroacetate and 88 wt% monobutyltin trichloride was produced in situ.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04731462 |
| 出典データセット | uspto-grants-1988_03 |
| ORD ID | ord-ea11274850b1410b946a121874bacbcd |
| 出典メモ | uspto-grants-1988_03 |