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HRID 569276作成日:2026年10月26日

Sulfamide → HCID 178479209、化合物

https://huagongshe.com/reaction/569276

反応式

関与物質

役割名称HCID仕込み量
反応物SulfamideHCID 82267—
反応物3-Chloropropionitrile hydrogen chlorideHCID 86742043—
溶媒Diethyl EtherHCID 3283—
生成物HCID 178479209HCID 178479209—

反応手順

To a stirred suspension of 9.61 g. (0.10 mole) of sulfamide in 30 ml (34 g., 0.38 mole) of 3-chloropropionitrile hydrogen chloride gas is introduced, as described in Example 1. After cooling with ice water for one hour the reaction mixture is diluted with 30 ml of dry ethyl ether, the product is filtered off, washed twice with acetone and dried.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US04731479
出典データセットuspto-grants-1988_03
ORD IDord-3edc6a87650c40d881e2ef0137c4c5f3
出典メモuspto-grants-1988_03