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Phthalic Anhydride → 2-{N,N-di(2-ethylhexyl)carbamoyl}-benzoic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Phthalic Anhydride | HCID 6811 | — |
| 反応物 | Bis(2-ethylhexyl)amine | HCID 7791 | — |
| 溶媒 | Acetonitrile | HCID 6342 | — |
| 生成物 | 2-{N,N-di(2-ethylhexyl)carbamoyl}-benzoic acid | HCID 20147052 | 100.2% |
反応手順
To 200 ml of acetonitrile were added 14.8 g of phthalic anhydride and 24.2 g of di(2-ethylhexyl)amine and the mixture was refluxed for 2 hours and then concentrated to provide 39.0 g of oily 2-{N,N-di(2-ethylhexyl)carbamoyl}-benzoic acid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04732845 |
| 出典データセット | uspto-grants-1988_03 |
| ORD ID | ord-05c4a1e5b7cb48eabc323ec2c396856b |
| 出典メモ | uspto-grants-1988_03 |