化工社化工社 化学情報印刷レポート · 研究参考用
Dimethylamine → 3-Hydroxy-N,N,2-trimethylbenzamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Dimethylamine | HCID 674 | — |
| 反応物 | 3-Hydroxy-2-methylbenzoic Acid | HCID 252023 | — |
| 生成物 | 3-Hydroxy-N,N,2-trimethylbenzamide | HCID 57753838 | 42% |
反応手順
The title compound was prepared from 3-hydroxy-2-methylbenzoic acid and dimethylamine, using the same method as that described for preparation 75, as a solid in 42% yield. 1H NMR (400 MHz, CDCl3) δ: 1.95 (s, 3H), 2.70 (s, 3H), 2.95 (s, 3H), 6.55 (d, 1H), 6.80 (d, 1H), 7.00 (m, 1H), 9.50 (s, 1H); LRMS APCI m/z 180 [M+H]+
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09023872B2 |
| 出典データセット | uspto-grants-2015_05 |
| ORD ID | ord-21988550690c4b0f8bb5cefb1ccba954 |
| 出典メモ | uspto-grants-2015_05 |