関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Furan | HCID 8029 | — |
| 反応物 | 1,4-Methanonaphthalene | HCID 56612571 | — |
| 生成物 | Pentacene | HCID 8671 | 40% |
反応手順
In summary, a new stable and soluble pentacene precursor 2 was synthesized in 40% yield from the cycloaddition of a furan derivative 3 and a benzonorbornadiene 4. Compound 2 releases a unit of CO upon heating at 128° C. or by irradiation with UV light (366 nm) to produce pentacene in nearly quantitative yield. Thin films of pentacene were prepared by spin-coating followed by thermal annealing, and found to display typical FET characteristics.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US09034439B2 |
|---|
| 出典データセット | uspto-grants-2015_05 |
|---|
| ORD ID | ord-dcfaaa3517ca4c8ea9c377fa52f530e3 |
|---|
| 出典メモ | uspto-grants-2015_05 |
|---|
