Methyl 2-isothiocyanato-4,5-dimethylthiophene-3-carboxylate → 2,3-dihydro-5,6-dimethyl-3-(3-(5-methyl-1H-imidazol-1-yl)propyl)-2-thioxothieno[2,3-d]pyrimidin-4(1H)-one
反応式
[N:1]([C:4]1[S:5][C:6]([CH3:14])=[C:7]([CH3:13])[C:8]=1[C:9]([O:11]C)=O)=[C:2]=[S:3].[CH3:15][C:16]1[N:20]([CH2:21][CH2:22][CH2:23][NH2:24])[CH:19]=[N:18][CH:17]=1>>[CH3:13][C:7]1[C:8]2[C:9](=[O:11])[N:24]([CH2:23][CH2:22][CH2:21][N:20]3[C:16]([CH3:15])=[CH:17][N:18]=[CH:19]3)[C:2](=[S:3])[NH:1][C:4]=2[S:5][C:6]=1[CH3:14]参加物
3
実験手順
The compound was synthesized starting from methyl 2-isothiocyanato-4,5-dimethylthiophene-3-carboxylate (0.1 g, 0.44 mmol) and 3-(5-methyl-1H-imidazol-1-yl)propan-1-amine (5) (0.06 g, 0.44 mmol) as described above.
後処理
- customThe compound was synthesized
出典と根拠
- ORDレコード
- ord-2c80f7661d4a4ddca993bdbacac2e0a9
- 出典データセット
- uspto-grants-2015_05
- 特許番号
- US09034907B2
反応ノート
読み込み中…