化工社化工社 化学情報印刷レポート · 研究参考用
3,5-Dimethyl-1-hexyn-3-ol → beta-CD Surfynol
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3,5-Dimethyl-1-hexyn-3-ol | HCID 61018 | — |
| 反応物 | beta-Cyclodextrin | HCID 444041 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | beta-CD Surfynol | HCID 131717491 | — |
反応手順
A mobile slurry is prepared by mixing about 410 g β-cyclodextrin and about 330 g deionized water (distilled water can be used) at about 25° C. in a stainless steel mixing bowl of a KitchenAid mixer using the flat beater mixing attachment. Mixing is continued while about 73 g of Perfume A is added rapidly. The low viscosity slurry immediately begins to thicken and becomes a stiff paste within a minute. Mixing is continued while 187 g of Surfynol 465 (supplied by Air Products) at about 25° C. is slowly added. This final composition is mixed until homogeneous for about 15 minutes.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05246611 |
| 出典データセット | uspto-grants-1993_09 |
| ORD ID | ord-faa192ddc81149e4a09422705fe2de84 |
| 出典メモ | uspto-grants-1993_09 |