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Triphenylborane → Butyl ethyl(3-aminopropyl)phosphinate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Triphenylborane | HCID 70400 | — |
| 反応物 | Butyl ethyl(2-methyl-3-aminopropyl)phosphinate | HCID 46212766 | — |
| 溶媒 | Toluene | HCID 1140 | — |
| 生成物 | Butyl ethyl(3-aminopropyl)phosphinate | HCID 46212699 | 216.6% |
反応手順
207 g (1 mol) of butyl ethyl(3-aminopropyl)phosphinate (produced as in Example 15) and 242 g (1 mol) of triphenylborane are stirred in 400 ml of toluene at room temperature for 1 hour. Toluene is distilled off at reduced pressure to leave 449 g (100% of theory) of butyl ethyl(3-aminopropyl)phosphinate as triphenylborane adduct.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09035088B2 |
| 出典データセット | uspto-grants-2015_05 |
| ORD ID | ord-c43a7e6d12634605955e22ca7a853a9c |
| 出典メモ | uspto-grants-2015_05 |