Carbon Dioxide → Cesium stearate
反応式
C([O-])([O-])=O.[Cs+:5].[Cs+].[C:7]([OH:26])(=[O:25])[CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH3:24].C(=O)=O>C(O)CCC>[C:7]([O-:26])(=[O:25])[CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH3:24].[Cs+:5]参加物
5
実験手順
A mixture of Cs2CO3 and stearic acid was added to butanol in the ratio 1:2 and kept at reflux temperature until no more CO2 formed. Subsequently, butanol was separated on the rotary evaporator, the residue mixed with ether and aspirated, m.p.:263-269° C.
後処理
- customformed
- customSubsequently, butanol was separated on the rotary evaporator
- additionthe residue mixed with ether
出典と根拠
- ORDレコード
- ord-89685cf973f9440c968721127bded328
- 出典データセット
- uspto-grants-2015_05
- 特許番号
- US09040112B2
反応ノート
読み込み中…