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Water → Adipic acid di(2-propylidene hydrazide)
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Water | HCID 962 | — |
| 反応物 | Adipic Dihydrazide | HCID 66117 | — |
| 溶媒 | Acetone | HCID 180 | — |
| 生成物 | Adipic acid di(2-propylidene hydrazide) | HCID 86666342 | — |
反応手順
In a stainless steel flask equipped with an agitator, 58.6 grams of water were added, the agitator was turned on, then 25 grams of adipic acid dihydrazide were added. The mixture was agitated for at least 10 minutes until a stable dispersion was formed. 16.4 grams of 2-propanone were then added under mixing. A clear solution formed after a few minutes. Mixing was continued for at least another hour until reaction product precipitated and formed a stable dispersion.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09040617B2 |
| 出典データセット | uspto-grants-2015_05 |
| ORD ID | ord-59e99d01d81845d1a2b7979ebe0a412e |
| 出典メモ | uspto-grants-2015_05 |