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HRID 5788作成日：2026年10月26日

1-Methylpiperazine → 2-Tert-butyl-6[(4-methylpiperazin-1-yl)thiocarbonylamino]-5-(4-methyl-piperazin-1-yl)benzothiazole

https://huagongshe.com/reaction/5788

反応式

関与物質

役割名称HCID仕込み量
反応物1-MethylpiperazineHCID 53167—
反応物2-Tert-butyl-6-isothiocyanato-5-(4-methyl-piperazin-1-yl)benzothiazoleHCID 19794187—
生成物2-Tert-butyl-6[(4-methylpiperazin-1-yl)thiocarbonylamino]-5-(4-methyl-piperazin-1-yl)benzothiazoleHCID 19794192—

反応手順

Using the procedure described in Example 1 by reaction of 2-tert-butyl-6-isothiocyanato-5-(4-methyl-piperazin-1-yl)benzothiazole with 4-methylpiperazine is obtained 2-tert-butyl-6[(4-methylpiperazin-1-yl)thiocarbonylamino]-5-(4-methyl-piperazin-1-yl)benzothiazole, melting at 190°-193°.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US05246927
出典データセットuspto-grants-1993_09
ORD IDord-c586dd8d365640deae3890d8575254f9
出典メモuspto-grants-1993_09