Stearic Acid → HCID 178485000、化合物

HRID 579848ノート

反応式

HRID 579848 の反応式
[O:1]=[C:2]1[O:8][C@H:7]([C@H:9]([CH2:11][OH:12])[OH:10])[C:5]([OH:6])=[C:3]1[OH:4].[CH3:13][C:14]1[NH:18][CH:17]=[N:16][C:15]=1[CH2:19][S:20][CH2:21][CH2:22]/[N:23]=[C:24](/[NH:27][C:28]#[N:29])\[NH:25][CH3:26].C(O)(=O)CCCCCCCCCCCCCCCCC>ClCCl>[CH3:13][C:14]1[NH:18][CH:17]=[N:16][C:15]=1[CH2:19][S:20][CH2:21][CH2:22]/[N:23]=[C:24](/[NH:27][C:28]#[N:29])\[NH:25][CH3:26].[O:1]=[C:2]1[O:8][C@H:7]([C@H:9]([CH2:11][OH:12])[OH:10])[C:5]([O-:6])=[C:3]1[OH:4]

参加物

5

反応物 3

HCID 5281Stearic AcidHCID 54670067L-Ascorbic AcidHCID 178484997HCID 178484997、化合物

生成物 1

HCID 178485000HCID 178485000、化合物

試薬・触媒・溶媒 1

HCID 6344Dichloromethane溶媒

実験手順

0.88 g (0.5 cmole) of ascorbic acid and 1.26 g (0.5 cmole) of cimetidine were added to a solution of stearic acid (2.14 g) in dichloromethane (q.s.). The mixture was filtered without washing and dried. Weight: 2.5 g. A stereoscopically homogenous white solid. Is unaltered by ambient conditions.

後処理

  1. filtrationThe mixture was filtered
  2. washwithout washing
  3. customdried

出典と根拠

ORDレコード
ord-121a47f47f65444b83c78d94312a0abd
出典データセット
uspto-grants-1988_06
特許番号
US04749790

反応ノート

読み込み中…