化工社化工社 化学情報印刷レポート · 研究参考用
Carnitine Chloride → (-)-Carnitine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Carnitine Chloride | HCID 5970 | — |
| 反応物 | 3-Hydroxy-4-(trimethylammonio)butanoate hydrochloride | HCID 9794197 | — |
| 反応物 | HCID 86742216 | HCID 86742216 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | (-)-Carnitine | HCID 10917 | 75% |
反応手順
The procedure of Example 8 was followed except that the concentration of DL-carnitine chloride for the F-2 stage was 50 g/l, which consisted of 8 parts of L-carnitine chloride and 2 parts of D-carnitine chloride. L-carnitine inner salt was isolated as before from 50 ml of the fermentation mixture (F-2 stage, 69 hours) [1.216 g (75% yield, [α]D25 -30.4°, c=2.8, H2O].
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04751182 |
| 出典データセット | uspto-grants-1988_06 |
| ORD ID | ord-ed064ba63b3b41c086f192ae043cb14d |
| 出典メモ | uspto-grants-1988_06 |