Hydrochloric Acid → HCID 20135785、化合物

HRID 580146ノート

反応式

HRID 580146 の反応式
[CH2:1]([N:3]([CH2:19][CH3:20])[CH2:4][CH2:5][CH2:6][NH:7][C:8]1[C:16]2[C:11](=[C:12]([NH2:18])[CH:13]=[C:14]([NH2:17])[CH:15]=2)[NH:10][N:9]=1)[CH3:2].[ClH:21].C(OCC)C>C(O)C>[ClH:21].[ClH:21].[ClH:21].[CH2:19]([N:3]([CH2:1][CH3:2])[CH2:4][CH2:5][CH2:6][NH:7][C:8]1[C:16]2[C:11](=[C:12]([NH2:18])[CH:13]=[C:14]([NH2:17])[CH:15]=2)[NH:10][N:9]=1)[CH3:20]

参加物

5

反応物 3

HCID 313Hydrochloric AcidHCID 3283Diethyl EtherHCID 20135762HCID 20135762、化合物

生成物 1

HCID 20135785HCID 20135785、化合物

試薬・触媒・溶媒 1

HCID 702Ethanol溶媒

実験手順

In 20 ml of absolute ethyl alcohol was dissolved 2.0 g of the 3-(3-diethylaminopropylamino)-5,7-diaminoindazole, and into the solution was introduced dried hydrogen chloride gas under cooling with ice. Then to the solution was added anhydrous diethyl ether to separate crystals. The crystals were obtained by filtration and dried to give 3-(3-diethylaminopropylamino)-5,7 -diaminoindazole trihydrochloride having the following analytical value.

後処理

  1. temperatureunder cooling with ice
  2. customto separate crystals
  3. customThe crystals were obtained by filtration
  4. customdried

出典と根拠

ORDレコード
ord-d9f6a2c067d04cfe83e4782c10e536bc
出典データセット
uspto-grants-1988_06
特許番号
US04751302

反応ノート

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