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Hydroquinone → Triphenylmethyl acrylate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Hydroquinone | HCID 785 | — |
| 反応物 | Trityl chloride | HCID 6456 | — |
| 反応物 | Potassium acrylate | HCID 4429391 | — |
| 溶媒 | Dimethylformamide | HCID 6228 | — |
| 生成物 | Triphenylmethyl acrylate | HCID 12641354 | — |
反応手順
1 mole triphenylchloromethane was stirred with 1.5 moles potassium acrylate in 998 g dimethyl formamide in the presence of 0.14 g hydroquinone under the conditions described in Example 1. The precipitated potassium chloride was filtered off and the triphenyl methyl acrylate solution was concentrated by rotary evaporation at 65° to 100° C. and reduced to produce liquid triphenylmethyl acrylate. This was dissolved at 70 percent in xylene and filtered.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04752629 |
| 出典データセット | uspto-grants-1988_06 |
| ORD ID | ord-7e5b6cf23b4a4a57b26e02bf28097737 |
| 出典メモ | uspto-grants-1988_06 |