関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Thionyl Chloride | HCID 24386 | — |
| 反応物 | HCID 178526157 | HCID 178526157 | — |
| 生成物 | Benzylthiocarbonyl chloride | HCID 19906501 | 92% |
反応手順
A quantity of 762 g (4.536 mol) of 2-phenylthioacetic acid is stirred at room temperature for 3 hours with thionyl chloride (375 ml, 5.14 mol), then stirred at 40° C. for 3 hours. Rotary evaporation followed by bulb-to-bulb distillation gives 777 g (4.166 mol, 92%) of 2-phenylthioacetyl chloride.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US05919951 |
|---|
| 出典データセット | uspto-grants-1999_07 |
|---|
| ORD ID | ord-e2aa14c9ba0f46cdbde657d3be99be68 |
|---|
| 出典メモ | uspto-grants-1999_07 |
|---|
