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HRID 581874作成日：2026年10月26日

5-Isopropyl-6-(3,5-dimethylphenyl)thio-2,4-pyrimidinedione → 1-{[3,4-Di(hydroxymethyl)cyclopent-1-en-1-yl]methyl}-5-isopropyl-6-(3,5-dimethylphenylthio)-2,4-pyrimidinedione

https://huagongshe.com/reaction/581874

反応式

関与物質

役割名称HCID仕込み量
反応物5-Isopropyl-6-(3,5-dimethylphenyl)thio-2,4-pyrimidinedioneHCID 10493727—
反応物[3,4-Di(t-butyldimethylsilyloxymethyl)cyclopent-1-en-1-yl]methyl bromideHCID 54350482—
生成物1-{[3,4-Di(hydroxymethyl)cyclopent-1-en-1-yl]methyl}-5-isopropyl-6-(3,5-dimethylphenylthio)-2,4-pyrimidinedioneHCID 6997759517.9%

反応手順

5-Isopropyl-6-(3,5-dimethylphenylthio)-2,4-pyrimidinedione and [3,4-di(t-butyldimethylsilyloxymethyl)cyclopent-1-en-1-yl]methyl bromide were reacted by the same method with example 28 to obtain the titled compound (51 mg).

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US05922727
出典データセットuspto-grants-1999_07
ORD IDord-1a1620b703ea43c086cba115d9b3d26b
出典メモuspto-grants-1999_07