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HRID 581878作成日：2026年10月27日

6-(3,5-Dimethyl-benzoyl)-5-isopropyl-1H-pyrimidine-2,4-dione → 1-{[3,4-Di(hydroxymethyl)cyclopent-1-en-1-yl]methyl}-5-isopropyl-6-(3,5-dimethylbenzoyl)-2,4-pyrimidinedione

https://huagongshe.com/reaction/581878

反応式

関与物質

役割名称HCID仕込み量
反応物6-(3,5-Dimethyl-benzoyl)-5-isopropyl-1H-pyrimidine-2,4-dioneHCID 22256582—
反応物[3,4-Di(t-butyldimethylsilyloxymethyl)cyclopent-1-en-1-yl]methyl bromideHCID 54350482—
生成物1-{[3,4-Di(hydroxymethyl)cyclopent-1-en-1-yl]methyl}-5-isopropyl-6-(3,5-dimethylbenzoyl)-2,4-pyrimidinedioneHCID 6997780726.3%

反応手順

5-Isopropyl-6-(3,5-dimethylbenzoyl)-2,4-pyrimidinedione and [3,4-di(t-butyldimethylsilyloxymethyl)cyclopent-1-en-1-yl]methyl bromide were reacted by the same method with example 28 to obtain the titled compound (74 mg).

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US05922727
出典データセットuspto-grants-1999_07
ORD IDord-0876341c625343e3aca665566e713242
出典メモuspto-grants-1999_07