化工社化工社 化学情報印刷レポート · 研究参考用
5-Isopropyl-6-(3,5-dimethylphenyl)thio-2,4-pyrimidinedione → 1-(2-Cyclopent-3-en-1-ylethyl)-6-(3,5-dimethylphenyl)sulfanyl-5-isopropyl-pyrimidine-2,4-dione
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 5-Isopropyl-6-(3,5-dimethylphenyl)thio-2,4-pyrimidinedione | HCID 10493727 | — |
| 反応物 | 2-(Cyclopent-3-en-1-yl)ethyl toluenesulfonate | HCID 86754221 | — |
| 生成物 | 1-(2-Cyclopent-3-en-1-ylethyl)-6-(3,5-dimethylphenyl)sulfanyl-5-isopropyl-pyrimidine-2,4-dione | HCID 45269075 | 34.8% |
反応手順
5-Isopropyl-6-(3,5-dimethylphenylthio)-2,4-pyrimidinedione and 2-(cyclopent 3-en-1-yl)ethyl toluenesulfonate were reacted by the same method with example 35 to obtain the titled compound (134 mg).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05922727 |
| 出典データセット | uspto-grants-1999_07 |
| ORD ID | ord-adbd1622bf1e41b9a63e8c60ac58fac9 |
| 出典メモ | uspto-grants-1999_07 |