Sulfuric Acid → 1-(4-amino-3-nitrophenyl)ethanone
反応式
[C:1]([C:4]1[CH:9]=[CH:8][C:7]([NH:10]C(=O)C)=[C:6]([N+:14]([O-:16])=[O:15])[CH:5]=1)(=[O:3])[CH3:2].S(=O)(=O)(O)O>O>[C:1]([C:4]1[CH:9]=[CH:8][C:7]([NH2:10])=[C:6]([N+:14]([O-:16])=[O:15])[CH:5]=1)(=[O:3])[CH3:2]参加物
4
実験手順
N-(4-acetyl-2-nitrophenyl)acetamide (26.5 g, 11,94 mmol) was added to a mixture of water and concentrated sulfuric acid, 150 ml (1:2). After 15 minutes the mixture was poured into water. The product was filtered off, washed with water and dried.
後処理
- filtrationThe product was filtered off
- washwashed with water
- customdried
出典と根拠
- ORDレコード
- ord-2920040f7e124e928047af60c67b4e0d
- 出典データセット
- uspto-grants-1999_07
- 特許番号
- US05922725
反応ノート
読み込み中…