関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Potassium Carbonate | HCID 11430 | — |
| 反応物 | 2,4,6-Trifluoropyridine | HCID 2783289 | — |
| 反応物 | HCID 178481859 | HCID 178481859 | — |
| 溶媒 | Sulfolane | HCID 31347 | — |
| 生成物 | 2,4,6-Tris(1-methyl-3-trifluoromethylpyrazol-5-yloxy)pyridine | HCID 15869678 | — |
反応手順
A stirred mixture of 2,4,6-trifluoropyridine (4.8 g, 36 mmol), 5-hydroxy-1-methyl-3-trifluoromethylpyrazole (19.8 g, 119 mmol) and potassium carbonate (18.1 g, 131 mmol) in anhydrous sulfolane (25 ml) is heated to 80° C. over a period of 3 days.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US05922738 |
|---|
| 出典データセット | uspto-grants-1999_07 |
|---|
| ORD ID | ord-2e3c5cffd801481fb6c6cb10484d4176 |
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| 出典メモ | uspto-grants-1999_07 |
|---|
