Hydrochloric Acid → HCID 70347532、化合物
反応式
[CH3:1][S:2]([C:5]1[CH:10]=[CH:9][C:8]([C:11]2[CH2:15][CH2:14][C:13](=[O:16])[C:12]=2[C:17]2[CH:18]=[N:19][CH:20]=[CH:21][CH:22]=2)=[CH:7][CH:6]=1)(=[O:4])=[O:3].[ClH:23]>C(Cl)Cl>[ClH:23].[CH3:1][S:2]([C:5]1[CH:10]=[CH:9][C:8]([C:11]2[CH2:15][CH2:14][C:13](=[O:16])[C:12]=2[C:17]2[CH:18]=[N:19][CH:20]=[CH:21][CH:22]=2)=[CH:7][CH:6]=1)(=[O:4])=[O:3]参加物
4
実験手順
To a solution of 3-(4-(methylsulfonyl)phenyl)-2-(3-pyridinyl)-2-cyclopenten-1-one (5.0 g, 15.96 mmol) in CH2Cl2 (50 mL) was passed a stream of HCl gas for 10 min. Excess HCl was removed by bubbling a stream of air through the solution. The solution was then concentrated and swished in Et2O to give 5.7 g of the title compound.
後処理
- customfor 10 min
- customExcess HCl was removed
- customby bubbling a stream of air through the solution
- concentrationThe solution was then concentrated
出典と根拠
- ORDレコード
- ord-d177aa9e1096408ea3a6d985ea612dd1
- 出典データセット
- uspto-grants-1999_07
- 特許番号
- US05922742
反応ノート
読み込み中…