化工社化工社 化学情報印刷レポート · 研究参考用
Methyl 5,6-Dichloronicotinate → Dimethyl 3-Chloro-2,6-pyridinedicarboxylate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Methyl 5,6-Dichloronicotinate | HCID 2782166 | — |
| 反応物 | 2,3-Dichloro-5-(methoxymethyl)pyridine | HCID 11137960 | — |
| 生成物 | Dimethyl 3-Chloro-2,6-pyridinedicarboxylate | HCID 53845654 | 73% |
反応手順
Example 2 was repeated, except that the 2,3-dichloro-5-(methoxymethyl)pyridine was replaced by the same molar amount of methyl 2,3-dichloro-5-pyridinecarboxylate. After a reaction time of 6 hours at a bath temperature of 160° C., 1.20 g (73 percent) of a yellow product was obtained. Other data concerning the product was:
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05925765 |
| 出典データセット | uspto-grants-1999_07 |
| ORD ID | ord-09075152a86f4f358289b2225de3bb1c |
| 出典メモ | uspto-grants-1999_07 |