Butyl bromide → 1-Butyl-4-(4-Methyl-3-nitro-phenyl)-piperazine

HRID 584062

反応式

HRID 584062 の反応式
[CH3:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]2[CH2:13][CH2:12][NH:11][CH2:10][CH2:9]2)=[CH:4][C:3]=1[N+:14]([O-:16])=[O:15].[CH2:17](Br)[CH2:18][CH2:19][CH3:20]>>[CH2:17]([N:11]1[CH2:10][CH2:9][N:8]([C:5]2[CH:6]=[CH:7][C:2]([CH3:1])=[C:3]([N+:14]([O-:16])=[O:15])[CH:4]=2)[CH2:13][CH2:12]1)[CH2:18][CH2:19][CH3:20]

参加物

3

反応物 2

HCID 8002Butyl bromideHCID 47388041-(4-Methyl-3-nitrophenyl)piperazine

生成物 1

HCID 223451931-Butyl-4-(4-Methyl-3-nitro-phenyl)-piperazine

実験手順

Beginning with 1-(4-methyl-3-nitro-phenyl)-piperazine and 1-butylbromide, the title compound was recovered by the procedure described in Example 2. MS m/z (rel. intensity, 70 eV) 277 (M+, 23), 234 (bp), 191 (17), 70 (64), 56 (33).

後処理

  1. customthe title compound was recovered by the procedure

出典と根拠

ORDレコード
ord-318be850ce3e4f99a2d62cd537508339
出典データセット
uspto-grants-2005_08
特許番号
US06924374B2

関連ノート

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