関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Succinic anhydride | HCID 7922 | — |
| 反応物 | HCID 178503197 | HCID 178503197 | — |
| 溶媒 | Dimethylformamide | HCID 6228 | — |
| 生成物 | 3-[3-(4-Methylsulfanyl-phenyl)-[1,2,4]oxadiazol-5-yl]-propionic acid | HCID 17122273 | — |
反応手順
Succinic anhydride (112 mg, 1.12 mmol) and N-hydroxy-4-methylsulfanyl-benzamidine (203 mg, 1.12 mmol) were dissolved in 2.0 mL of DMF and heated at 120° C. overnight. The cooled solution was evaporated and dried to give 3-[3-(4-methylsulfanyl-phenyl)-[1,2,4]oxadiazol-5-yl]-propionic acid which was used without further purification.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US06924284B2 |
|---|
| 出典データセット | uspto-grants-2005_08 |
|---|
| ORD ID | ord-1c92a610d92b49ddaf94ad9316aee7bc |
|---|
| 出典メモ | uspto-grants-2005_08 |
|---|
