化工社化工社 化学情報印刷レポート · 研究参考用
Triisopropyl borate → 5-[1,3]Dioxolan-2-yl-2-methylphenylboronic acid
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Triisopropyl borate | HCID 21531 | — |
| 反応物 | 1,3-Dioxolane, 2-(3-bromo-4-methylphenyl)- | HCID 11241979 | — |
| 生成物 | 5-[1,3]Dioxolan-2-yl-2-methylphenylboronic acid | HCID 22345636 | — |
反応手順
In a manner similar to that of Example 2(k), by reacting 11.1 g (46 mmol) of 2-(3-bromo-4-methylphenyl)[1,3]dioxolane with 12.3 ml (55 mmol) of triisopropyl borate, 6 g (88%) of product are obtained in the form of an oil.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06924400B2 |
| 出典データセット | uspto-grants-2005_08 |
| ORD ID | ord-d41da316721d4ee38d4763bbf5e49684 |
| 出典メモ | uspto-grants-2005_08 |