4-Fluorophenylboronic acid → HCID 22337836、化合物
反応式
Br[C:2]1[CH:27]=[CH:26][C:5]([CH2:6][O:7][C:8]2[CH:17]=[CH:16][CH:15]=[C:14]3[C:9]=2[CH:10]=[CH:11][C:12]([NH:18][S:19]([C:22]([F:25])([F:24])[F:23])(=[O:21])=[O:20])=[CH:13]3)=[CH:4][CH:3]=1.[F:28][C:29]1[CH:34]=[CH:33][C:32](B(O)O)=[CH:31][CH:30]=1>CS(C)=O>[F:28][C:29]1[CH:34]=[CH:33][C:32]([C:2]2[CH:3]=[CH:4][C:5]([CH2:6][O:7][C:8]3[CH:17]=[CH:16][CH:15]=[C:14]4[C:9]=3[CH:10]=[CH:11][C:12]([NH:18][S:19]([C:22]([F:23])([F:25])[F:24])(=[O:21])=[O:20])=[CH:13]4)=[CH:26][CH:27]=2)=[CH:31][CH:30]=1参加物
4
実験手順
The title compound was prepared from the product of Example 1 and 4-florophenyl boronic acid according to the procedure of Example 2, m.p. 139-140° C. DMSO: δ 12.0 broad (s, 1H), 7.0-8.3(m, 14H, arom), 5.36 (s, 2H). CHN 60.63, 3.60, 2.94. Found 60.60, 3.50, 2.83.
出典と根拠
- ORDレコード
- ord-c94aca9660e4445bbc6084e8a48954b3