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2,5-Dimethylbenzaldehyde → [5-(2,5-Dimethyl-phenyl)-imidazo[1,2-b][1,2,4]triazol-6-yl]-(1,1,3,3-tetramethyl-butyl)-amine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2,5-Dimethylbenzaldehyde | HCID 22015 | — |
| 反応物 | 1,1,3,3-Tetramethylbutyl isocyanide | HCID 26725 | — |
| 反応物 | HCID 178418311 | HCID 178418311 | — |
| 溶媒 | Perchloric Acid | HCID 24247 | — |
| 生成物 | [5-(2,5-Dimethyl-phenyl)-imidazo[1,2-b][1,2,4]triazol-6-yl]-(1,1,3,3-tetramethyl-butyl)-amine | HCID 22335552 | — |
反応手順
Compound 54 was prepared in accordance with the general synthesis instructions from 1.0 ml (0.1 mmol) 3-amino-1,2,4-triazole solution (0.1 M, MC), 0.575 ml (0.115 mmol) 1,1,3,3-tetramethylbutylisonitrile solution (0.2 M, MC), 0.500 ml (0.15 mmol) 2,5-dimethylbenzaldehyde solution (0.3 M, MC) and 10 μl perchloric acid (w=20%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06936631B2 |
| 出典データセット | uspto-grants-2005_08 |
| ORD ID | ord-42a21424edf54702ac088341799fa885 |
| 出典メモ | uspto-grants-2005_08 |