Morpholine → HCID 178513121、化合物
反応式
I.[NH:2]([C:4](SC)=[NH:5])[NH2:3].[NH:8]1[CH2:13][CH2:12][O:11][CH2:10][CH2:9]1>CO>[N:8]1([C:4](=[NH:5])[NH:2][NH2:3])[CH2:13][CH2:12][O:11][CH2:10][CH2:9]1参加物
4
実験手順
To a solution of methyl hydrazinecarbimidothioate hydroiodide (0.100 g, 0.429 mmol) in MeOH (2 mL) was added morpholine (0.075 mL, 0.858 mmol) and refluxed overnight. Reaction was cool to RT and concentrated to get morpholine-4-carboximidhydrazide as a white solid in quantitative yield.
後処理
- temperaturerefluxed overnight
- customReaction
- concentrationconcentrated
出典と根拠
- ORDレコード
- ord-6407090cb11347459dd3c8c7f1ae4f0f
- 出典データセット
- uspto-grants-2016_01
- 特許番号
- US09227971B2
反応ノート
読み込み中…