Methyl 3-amino-2-methylpropanoate hydrochloride → Methyl 1-(aminomethyl)cyclopropane-1-carboxylate--hydrogen chloride (1/1)
反応式
[ClH:1].[NH2:2][CH2:3][CH:4]([CH3:9])[C:5]([O:7][CH3:8])=[O:6].N[CH2:11]C1(C(O)=O)CC1>>[ClH:1].[NH2:2][CH2:3][C:4]1([C:5]([O:7][CH3:8])=[O:6])[CH2:11][CH2:9]1参加物
3
実験手順
The title compound was prepared in analogy to Compound W in Example 20 by using 1-(aminomethyl)cyclopropanecarboxylic acid (CAS number: 139132-50-6, J&K; for its synthesis, please refer to: Mertin A., et al. Synlett, 1991, 2, 87-9) instead of DL-3-aminoisobutyric acid.
出典と根拠
- ORDレコード
- ord-371ed32666a142eca0c49046322d6718
- 出典データセット
- uspto-grants-2016_01
- 特許番号
- US09233978B2
反応ノート
読み込み中…