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(R)-2-amino-3-(4-ethoxy-phenyl)-propionic acid hydrochloride → O-Ethyl-D-tyrosine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | (R)-2-amino-3-(4-ethoxy-phenyl)-propionic acid hydrochloride | HCID 71185515 | — |
| 反応物 | (R)-2-Butoxycarbonylamino-3-(4-ethoxy-phenyl)-propionic acid | HCID 71186057 | — |
| 溶媒 | Hydrochloric Acid | HCID 313 | — |
| 溶媒 | 1,4-Dioxane | HCID 31275 | — |
| 生成物 | O-Ethyl-D-tyrosine | HCID 18596379 | — |
反応手順
(R)-2-Butoxycarbonylamino-3-(4-ethoxy-phenyl)-propionic acid (4.0 g, 12.93 mmol) was dissolved in 4M HCl in dioxan (150 mL). After one hour at room temperature the solvent was removed in vacuo to give a white solid identified as (R)-2-amino-3-(4-ethoxy-phenyl)-propionic acid hydrochloride (3.18 g, 12.9 mmol, 100%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09234000B2 |
| 出典データセット | uspto-grants-2016_01 |
| ORD ID | ord-58046c4116bc4c01b67c80427d010a57 |
| 出典メモ | uspto-grants-2016_01 |