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Thionyl Chloride → N-(2-chloro-4-(perfluoropropan-2-yl)-6-(trifluoromethyl)phenyl)-4-iodo-3-nitrobenzamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Thionyl Chloride | HCID 24386 | — |
| 反応物 | 4-Iodo-3-nitrobenzoic acid | HCID 11208598 | — |
| 反応物 | 2-Chloro-4-(perfluoropropan-2-yl)-6-(trifluoromethyl)aniline | HCID 58297418 | — |
| 反応物 | 4-Iodo-3-nitrobenzoyl chloride | HCID 58932935 | — |
| 生成物 | N-(2-chloro-4-(perfluoropropan-2-yl)-6-(trifluoromethyl)phenyl)-4-iodo-3-nitrobenzamide | HCID 86654250 | — |
反応手順
According to the method of 1-3 of Example 1, a target compound was prepared from 4-iodo-3-nitrobenzoyl chloride prepared from 4-iodo-3-nitrobenzoic acid and thionyl chloride, and 2-chloro-4-(perfluoropropan-2-yl)-6-(trifluoromethyl)aniline.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09237745B2 |
| 出典データセット | uspto-grants-2016_01 |
| ORD ID | ord-f95d50db96684ba6b950c4d83e7ced37 |
| 出典メモ | uspto-grants-2016_01 |