関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Dimethylformamide | HCID 6228 | — |
| 反応物 | 3-Pyridinecarbonyl chloride, hydrochloride (1:1) | HCID 88438 | — |
| 反応物 | Aluminum(III) Chloride | HCID 6451240 | — |
| 反応物 | Benzoselenazolinone | HCID 87879929 | — |
| 生成物 | 6-Nicotinoylbenzoselenazolinone | HCID 131718174 | — |
反応手順
9.9 ml (0.13 mol) of dimethylformamide are introduced dropwise and with stirring into a 250-ml flask containing 61.3 g (0.46 mol) of aluminum chloride, and the flask is fitted with a reflux condenser and heated in an oil bath to a temperature in the region of 45° C. 7.9 g (0.04 mol) of benzoselenazolinone and 10.6 g (0.06 mol) of nicotinoyl chloride hydrochloride are introduced.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US05246951 |
|---|
| 出典データセット | uspto-grants-1993_09 |
|---|
| ORD ID | ord-e84ede7fe7a54153a4005eb838402408 |
|---|
| 出典メモ | uspto-grants-1993_09 |
|---|
