関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Sodium Chloride | HCID 5234 | — |
| 反応物 | Ethylenediaminetetraacetic Acid | HCID 6049 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | EDTA disodium salt | HCID 8759 | — |
反応手順
Crude MTC product (MW 373.90, 10.0 g, ˜26.7 mmol) was fully dissolved in H2O (270 cm3). Ethylenediaminetetraacetic acid (EDTA) disodium salt dihydrate (MW 372.24, 1 g, 2.68 mmol, 0.1 equivalents) was added. The mixture was stirred at 65° C. for approximately 1 hour. The mixture was filtered by vacuum filtration. The filtrate was collected. Sodium chloride (NaCl, MW 57.96, 16 g, 0.276 mol, 10 equivalents) was added to the filtrate while stirring. The resulting precipitate was collected by vacuum filtration.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US09242946B2 |
|---|
| 出典データセット | uspto-grants-2016_01 |
|---|
| ORD ID | ord-24ff0427a43947f48c65db3449de5a0a |
|---|
| 出典メモ | uspto-grants-2016_01 |
|---|
