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3-Chloro-4-methylaniline → (3-Chloro-4-methylphenyl)hydrazine
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3-Chloro-4-methylaniline | HCID 7255 | — |
| 反応物 | Stannous chloride dihydrate | HCID 61436 | — |
| 反応物 | Sodium Nitrite | HCID 23668193 | — |
| 溶媒 | Hydrochloric Acid | HCID 313 | — |
| 生成物 | (3-Chloro-4-methylphenyl)hydrazine | HCID 292017 | 68,412.602% |
反応手順
The title compound was prepared according to the procedure described in step-1 of Intermediate-61 by using 3-chloro-4-methylaniline (6.0 g, 0.0420 mmol), NaNO2 (8.56 g, 0.050 mmol), SnCl2.2H2O (23.7 g, 0.105 mmol) and conc. HCl (100 mL) to afford 4.5 g of the desired product.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09439890B2 |
| 出典データセット | uspto-grants-2016_09 |
| ORD ID | ord-e122a62c34bf4e92874365984c726a1c |
| 出典メモ | uspto-grants-2016_09 |