Methyl 5-amino-5-(2,6-dimethoxyphenyl)pentanoate → HCID 69082749、化合物
反応式
[NH2:1][CH:2]([C:10]1[C:15]([O:16][CH3:17])=[CH:14][CH:13]=[CH:12][C:11]=1[O:18][CH3:19])[CH2:3][CH2:4][CH2:5][C:6]([O:8]C)=O.[S:20]1[C:24]([C:25]2[CH:26]=[C:27]([CH:30]=[CH:31][CH:32]=2)[CH:28]=O)=[CH:23][N:22]=[CH:21]1>>[CH3:19][O:18][C:11]1[CH:12]=[CH:13][CH:14]=[C:15]([O:16][CH3:17])[C:10]=1[CH:2]1[N:1]([CH2:28][C:27]2[CH:30]=[CH:31][CH:32]=[C:25]([C:24]3[S:20][CH:21]=[N:22][CH:23]=3)[CH:26]=2)[C:6](=[O:8])[CH2:5][CH2:4][CH2:3]1参加物
3
実験手順
Prepared according to the described general procedure 1 (GP1) by reaction of methyl 5-amino-5-(2,6-dimethoxyphenyl)pentanoate with 3-(thiazol-5-yl)benzaldehyde. Subsequent purification by preparative HPLC afforded the target compound. LC-MS (conditions A): tR=0.78 min.; [M+H]+: 409.08 g/mol.
後処理
- customPrepared
- customSubsequent purification by preparative HPLC
- customafforded the target compound
出典と根拠
- ORDレコード
- ord-e969f13212d34806b9062ef372ea1bed