化工社化工社 化学情報印刷レポート · 研究参考用
2-Methoxybenzaldehyde → 6-(2-Methoxyphenyl)-1-(naphthalen-2-ylmethyl)piperidin-2-one
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Methoxybenzaldehyde | HCID 8658 | — |
| 反応物 | 1-(2-Naphthyl)methanamine | HCID 137282 | — |
| 生成物 | 6-(2-Methoxyphenyl)-1-(naphthalen-2-ylmethyl)piperidin-2-one | HCID 69083719 | — |
反応手順
Prepared according to the described general procedure 6 (GP6) with commercially available naphthalen-2-ylmethanamine and commercially available 2-methoxybenzaldehyde. Subsequent purification by preparative HPLC afforded the target compound. LC-MS (conditions H): tR=1.35 min.; [M+H]+: 346.35 g/mol.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09242970B2 |
| 出典データセット | uspto-grants-2016_01 |
| ORD ID | ord-c4629de8fb0b4ddba7066b267e92a1bb |
| 出典メモ | uspto-grants-2016_01 |