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2,6-Dimethoxybenzaldehyde → 6-(2,6-Dimethoxyphenyl)-1-(naphthalen-2-ylmethyl)piperidin-2-one
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2,6-Dimethoxybenzaldehyde | HCID 96404 | — |
| 反応物 | 1-(2-Naphthyl)methanamine | HCID 137282 | — |
| 生成物 | 6-(2,6-Dimethoxyphenyl)-1-(naphthalen-2-ylmethyl)piperidin-2-one | HCID 69082306 | — |
反応手順
Prepared according to the described general procedure 6 (GP6) with commercially available naphthalen-2-ylmethanamine and commercially available 2,6-dimethoxybenzaldehyde. Subsequent purification by preparative HPLC afforded the target compound. LC-MS (conditions H): tR=1.35 min.; [M+H]+: 375.79 g/mol.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09242970B2 |
| 出典データセット | uspto-grants-2016_01 |
| ORD ID | ord-0d1651c645b5490f981780cc2d70909e |
| 出典メモ | uspto-grants-2016_01 |