化工社化工社 化学情報印刷レポート · 研究参考用
Isoprene → Isoprene acrylonitrile
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Isoprene | HCID 6557 | — |
| 反応物 | Acrylonitrile | HCID 7855 | — |
| 生成物 | Isoprene acrylonitrile | HCID 168239 | — |
反応手順
Then, were added thereto 136 parts of isoprene and 0.37 part of methyl α-chlorophenyl acetate as an organic halide, and stirred under heating at 80° C. After a reaction for 17 hours, the same post-treatment as in Example 1 was carried out-to give a random (isoprene/acrylonitrile) copolymer. The conversion rate of isoprene was 31% and the conversion rate of acrylonitrile was 35%. The analysis results of the random (isoprene/acrylonitrile) polymer obtained are shown in Table 3. The polymer was confirmed to have a chlorine atom at the terminal of the polymer chain.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09243100B2 |
| 出典データセット | uspto-grants-2016_01 |
| ORD ID | ord-520eab6c62de4662875dc96321fa3706 |
| 出典メモ | uspto-grants-2016_01 |