関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Isoprene | HCID 6557 | — |
| 反応物 | 2-Chloropropionitrile | HCID 519225 | — |
| 生成物 | Isoprene acrylonitrile | HCID 168239 | — |
反応手順
Then, were added thereto 68.2 parts of isoprene and 1.79 parts of 2-chloropropionitrile as an organic halide and stirred under heating at 80° C. to conduct a polymerization reaction. After 137 hours, the same post-treatment as in Example 1 was carried out to give a random (isoprene/acrylonitrile) copolymer. The conversion rate of isoprene was 84% and the conversion rate of acrylonitrile was 79%. The analysis results of the random (isoprene/acrylonitrile) polymer obtained are shown in Table 3. The polymer was confirmed to have a chlorine atom at the terminal of the polymer chain.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 特許番号 | US09243100B2 |
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| 出典データセット | uspto-grants-2016_01 |
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| ORD ID | ord-60e0a25855b74722ac70ab07752689e7 |
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| 出典メモ | uspto-grants-2016_01 |
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