化工社化工社 化学情報印刷レポート · 研究参考用
Chloride → N,N-Dimethyl-N-(prop-2-en-1-yl)hexadecan-1-aminium chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Chloride | HCID 312 | — |
| 反応物 | Allyl chloride | HCID 7850 | — |
| 反応物 | Dimethylhexadecylamine | HCID 16221 | — |
| 生成物 | N,N-Dimethyl-N-(prop-2-en-1-yl)hexadecan-1-aminium chloride | HCID 20503036 | — |
反応手順
Allyl hexadecyl dimethyl ammonium chloride was prepared by reacting allyl chloride and dimethyl hexadecyl amine as set forth in Example 1. 17.8 grams of the chloride in 23.5% aqueous solution were treated with a stoichiometric excess of AgF in aqueous solution until analysis of the filtrate showed only a trace of chloride ion present. Excess silver ion was removed by the careful addition of NaCl, AgCl being removed by filtration.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04011259 |
| 出典データセット | uspto-grants-1977_03 |
| ORD ID | ord-a17a8510cadc46f49c66ddc06659ad6c |
| 出典メモ | uspto-grants-1977_03 |