Chloride → N,N-Dimethyl-N-(prop-2-en-1-yl)hexadecan-1-aminium chloride

HRID 596540

反応式

HRID 596540 の反応式
[CH2:1]([Cl:4])[CH:2]=[CH2:3].[CH3:5][N:6]([CH3:23])[CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22].[Cl-]>>[Cl-:4].[CH2:1]([N+:6]([CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22])([CH3:5])[CH3:23])[CH:2]=[CH2:3]

参加物

4

反応物 3

HCID 312ChlorideHCID 7850Allyl chlorideHCID 16221Dimethylhexadecylamine

生成物 1

HCID 20503036N,N-Dimethyl-N-(prop-2-en-1-yl)hexadecan-1-aminium chloride

実験手順

Allyl hexadecyl dimethyl ammonium chloride was prepared by reacting allyl chloride and dimethyl hexadecyl amine as set forth in Example 1. 17.8 grams of the chloride in 23.5% aqueous solution were treated with a stoichiometric excess of AgF in aqueous solution until analysis of the filtrate showed only a trace of chloride ion present. Excess silver ion was removed by the careful addition of NaCl, AgCl being removed by filtration.

後処理

  1. customExcess silver ion was removed by the careful addition of NaCl, AgCl being
  2. customremoved by filtration

出典と根拠

ORDレコード
ord-a17a8510cadc46f49c66ddc06659ad6c
出典データセット
uspto-grants-1977_03
特許番号
US04011259

関連ノート

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