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Bromomethyl 4-methoxyphenyl ketone → N-(4-chlorophenacyl) pyridazinium chloride
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Bromomethyl 4-methoxyphenyl ketone | HCID 4965 | — |
| 反応物 | Pyridazine | HCID 9259 | — |
| 反応物 | 2,4'-Dichloroacetophenone | HCID 70298 | — |
| 溶媒 | Pyridine | HCID 1049 | — |
| 生成物 | N-(4-chlorophenacyl) pyridazinium chloride | HCID 86734540 | — |
反応手順
Employing the procedure of Example I but replacing pyridine with a substantially equimolecular amount of pyridazine and replacing 4-methoxyphenacyl bromide with a substantially equimolecular amount of 4-chlorophenacyl chloride there is obtained N-(4-chlorophenacyl) pyridazinium chloride, a solid soluble in water.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | USRE029153 |
| 出典データセット | uspto-grants-1977_03 |
| ORD ID | ord-6e87b6dd681d4db6920a8772c4d5d4ea |
| 出典メモ | uspto-grants-1977_03 |