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HRID 596813作成日:2026年10月25日

Propylamine → 2-methyl-N-propylalaninamide

https://huagongshe.com/reaction/596813

反応式

関与物質

役割名称HCID仕込み量
反応物PropylamineHCID 7852—
反応物Methyl 2-amino-2-methylpropanoateHCID 4186341—
溶媒MethanolHCID 887—
生成物2-methyl-N-propylalaninamideHCID 21448036—

反応手順

To a solution of 26.3 parts of methyl 2-amino-2-methylpropionate in methanol is added 70 parts of n-propylamine. The mixture is placed in a bomb and left at a temperature of 100° C. for one week. The solvents are then stripped off under reduced pressure. Distillation of the residual oil affords N1 -propyl-2-amino-2-methylpropionamide, boiling at 58° C. at 0.1 mm pressure.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US04012367
出典データセットuspto-grants-1977_03
ORD IDord-065463928e104051adfab8401ac48500
出典メモuspto-grants-1977_03