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Propylamine → 2-methyl-N-propylalaninamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Propylamine | HCID 7852 | — |
| 反応物 | Methyl 2-amino-2-methylpropanoate | HCID 4186341 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | 2-methyl-N-propylalaninamide | HCID 21448036 | — |
反応手順
To a solution of 26.3 parts of methyl 2-amino-2-methylpropionate in methanol is added 70 parts of n-propylamine. The mixture is placed in a bomb and left at a temperature of 100° C. for one week. The solvents are then stripped off under reduced pressure. Distillation of the residual oil affords N1 -propyl-2-amino-2-methylpropionamide, boiling at 58° C. at 0.1 mm pressure.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04012367 |
| 出典データセット | uspto-grants-1977_03 |
| ORD ID | ord-065463928e104051adfab8401ac48500 |
| 出典メモ | uspto-grants-1977_03 |