化工社化工社 化学情報印刷レポート · 研究参考用
N-t-butoxycarbonyl-L-tryptophanyl-L-methionyl-L-aspartyl-D-alanine amide → N-t-butoxycarbonyl-L-tryptophanyl-L-methionyl-L-aspartyl-N1-propyl-2-amino-2-methylpropionamide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | N-t-butoxycarbonyl-L-tryptophanyl-L-methionyl-L-aspartyl-D-alanine amide | HCID 22796331 | — |
| 反応物 | L-methionyl-L-aspartyl-N1-propyl-2-amino-2-methylpropionamide hydrochloride hydrate | HCID 131710669 | — |
| 生成物 | N-t-butoxycarbonyl-L-tryptophanyl-L-methionyl-L-aspartyl-N1-propyl-2-amino-2-methylpropionamide | HCID 131710668 | — |
反応手順
When an equivalent quantity of L-methionyl-L-aspartyl-N1 -propyl-2-amino-2-methylpropionamide hydrochloride hydrate is substituted for the L-methionyl-L-aspartyl-D-alanine amide hydrochloride of Example 6, and the procedure detailed therein substantially repeated, there is obtained N-t-butoxycarbonyl-L-tryptophanyl-L-methionyl-L-aspartyl-N1 -propyl-2-amino-2-methylpropionamide hydrated with 2/3 mole of water per mole. Actual elemental analysis shows C: 55.82%; H: 7.21%; N: 12.37% and S: 4.72%. Theoretical elemental analysis is C: 55.79%; H: 7.22%; N: 12.20% and S: 4.66%. This compound is represented by the following formula. ##STR17##
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04012367 |
| 出典データセット | uspto-grants-1977_03 |
| ORD ID | ord-5e54c9aa9fb34732b7e0d633c727d277 |
| 出典メモ | uspto-grants-1977_03 |