化工社化工社 化学情報印刷レポート · 研究参考用
Benzeneacetonitrile, 4-methoxy- → 3-(4-Methoxy-phenyl)-5-[2-(4-methoxy-phenyl)-2H-pyrazol-3-yl]-benzo[c]isoxazole
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Benzeneacetonitrile, 4-methoxy- | HCID 66031 | — |
| 反応物 | 1-(4-methoxy-phenyl)-5-(4-nitro-phenyl)-1H-pyrazole | HCID 90032750 | — |
| 生成物 | 3-(4-Methoxy-phenyl)-5-[2-(4-methoxy-phenyl)-2H-pyrazol-3-yl]-benzo[c]isoxazole | HCID 73053292 | — |
反応手順
The title compound, yellow solid (7 mg, 5%), MS (ISP) m/z=398.2 [(M+H)+], mp 133° C., was prepared in accordance with the general method of example 1 from 1-(4-methoxy-phenyl)-5-(4-nitro-phenyl)-1H-pyrazole (intermediate G) (100 mg, 353 μmol) and commercially available 2-(4-methoxy-phenyl)-acetonitrile.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US09440962B2 |
| 出典データセット | uspto-grants-2016_09 |
| ORD ID | ord-4cbfde173a334afc80725cf1b6d0aeed |
| 出典メモ | uspto-grants-2016_09 |