戻る
化工社化工社 化学情報印刷レポート · 研究参考用
HRID 599724作成日:2026年10月27日

Oxygen → 4-Phenyl-3-Buten-2-one

https://huagongshe.com/reaction/599724

反応式

関与物質

役割名称HCID仕込み量
反応物OxygenHCID 977—
反応物4-Phenylbut-3-en-2-olHCID 15172—
触媒PlatinumHCID 23939—
溶媒WaterHCID 962—
生成物4-Phenyl-3-Buten-2-oneHCID 1590987.5%

反応手順

In an ambient pressure oxygen atmosphere, 29.2 mg of 4-phenyl-but-3-ene-2-ol and 33.9 mg of the platinum catalyst obtained in Example 1 were agitated for fifteen hours at 60° C. in 2 ml of water. The reaction mixture was subsequently extracted using ethyl acetate, and the organic layer was dried using magnesium sulfate, filtered and concentrated to obtain 25.2 mg (87% yield) of benzalacetone. The reaction equation and the analytical results of the product are shown below.

情報源と証拠

DOI10.6084/m9.figshare.5104873.v1
特許番号US07897817B2
出典データセットuspto-grants-2011_03
ORD IDord-441a9e81c2ae40b4b5312c7d92167e28
出典メモuspto-grants-2011_03