化工社化工社 化学情報印刷レポート · 研究参考用
2-Hydroxybenzonitrile → O-2-cyanophenyl dimethylthiocarbamate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-Hydroxybenzonitrile | HCID 11907 | — |
| 反応物 | Potassium Hydroxide | HCID 14797 | — |
| 反応物 | Dimethylthiocarbamoyl chloride | HCID 27871 | — |
| 生成物 | O-2-cyanophenyl dimethylthiocarbamate | HCID 14795403 | 94% |
反応手順
If the procedure described in Preparation XVI is followed starting from 15 g (126.10-3 mol) of 2-hydroxybenzonitrile, 17.9 g (145.10-3 mol) of dimethylthiocarbamoyl chloride and 7.4 g (126.10-3 mol) of potassium hydroxide, 24.1 g (yield: 94%) of the expected product are obtained.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05246961 |
| 出典データセット | uspto-grants-1993_09 |
| ORD ID | ord-0e3bf4991a3f466d9c41ae0105fc4554 |
| 出典メモ | uspto-grants-1993_09 |