化工社化工社 化学情報印刷レポート · 研究参考用
Ammonia → N-Amylurea
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ammonia | HCID 222 | — |
| 反応物 | Pentane, 1-isocyanato- | HCID 206036 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | N-Amylurea | HCID 198194 | — |
反応手順
To a 7.0 M solution of ammonia in methanol (32 mL) was dropwise added 1-isocyanatopentane (5.0 g, 0.044 mol). After the addition, the mixture was stirred at room temperature for 1 h and concentrated under reduced pressure to give a white solid, which was directly used for next step without further purification. LCMS calculated for C6H15N2O (M+H): 131.1. found 131.1.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07902205B2 |
| 出典データセット | uspto-grants-2011_03 |
| ORD ID | ord-23d6f2bf577e4920b65514a6eac45681 |
| 出典メモ | uspto-grants-2011_03 |