化工社化工社 化学情報印刷レポート · 研究参考用
Pentafluoroaniline → 501670-16-2
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Pentafluoroaniline | HCID 13040 | — |
| 反応物 | 3,5-Di-tert-butylsalicylaldehyde | HCID 688023 | — |
| 反応物 | 2,4-Bis(tert-butyl)-6-[[(2,6-dibromophenyl)imino]methyl]phenol | HCID 136346710 | — |
| 生成物 | 501670-16-2 | HCID 135509894 | — |
反応手順
Employing an analogous procedure to that described above for the synthesis of 2,4-bis(tert-butyl)-6-[[(2,6-dibromophenyl)imino]methyl]phenol, 2,3,4,5,6-pentafluoroaniline (0.54 g, 2.9 mmol) was added to 3,5-di-tert-butyl-2-hydroxybenzaldehyde (0.70 g, 2.9 mmol). The product was purified by recrystallisation from hot MeOH and isolated as yellow crystals.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07902308B2 |
| 出典データセット | uspto-grants-2011_03 |
| ORD ID | ord-1224c7f7869c44258aeb252783b2e5e7 |
| 出典メモ | uspto-grants-2011_03 |